Publications [#62745] of Tuan Vo-Dinh

Papers Published

  1. Capitan-Vallvey, L.F. and Ojeda, F. and Del Olmo, M. and Avidad, R. and Navalon, A. and Vo-Dinh, T., Use of transmitted room-temperature phosphorescence to improve nalidixic acid determination, Applied Spectroscopy, vol. 52 no. 1 (1998), pp. 101 - 105
    (last updated on 2007/04/14)

    Abstract:
    A method for nalidixic acid (NA) determination by transmitted room-temperature phosphorescence is proposed. The antibacterial agent NA in acidic solution shows native fluorescence; when NA is spotted on a filter paper precoated with β-cyclodextrin and lead (II) acetate and dried for 5 min, phosphorescence results. The transmitted phosphorescence was measured directly with the use of a homemade sample holder. The excitation and emission wavelengths were 330 and 417 nm, respectively. The applicable concentration range was between 0.06 and 4.50 µg/mL with a relative standard deviation of 2.8% and a detection limit of 0.02 µg/mL. The method was applied to the determination of NA in human urine and pharmaceuticals, with recoveries from 97.5 to 105.5%.

    Keywords:
    Phosphorescence;Fluorescence;Lead compounds;Body fluids;Drug products;